Journal of New Technology and Materials
Volume 3, Numéro 2, Pages 14-28
2013-12-28
Effect Of Surfactants In The Synthesis Of Nio Nanoparticles By Colloidal Thermal Assisted Reflux Condensation Method
Authors : Mohamed Jaffer Sadiq M. . Samson Nesaraj A .
Abstract
Nickel oxide (NiO) nanoparticles were prepared by colloidal thermal assisted reflux condensation method using nickel acetate (precursor salt) and N, N - Dimethylformamide - DMF (solvent) with or without the addition of surfactants such as cetyl trimethyl ammonium bromide (CTAB), polyvinyl pyrrolidone (PVP), polyvinyl alcohol (PVA) and sodium monododecyl sulphate (SDS) respectively. Finally, the prepared samples products were calcined at different temperatures systematically such as at 200oC, 400oC, 600oC, 800oC for 2 hrs each to get the phase pure product. The calcined nanoparticles were characterized by X-Ray Diffraction (XRD), Energy Dispersive X-ray Analysis (EDAX), Fourier Transform Infrared (FTIR) Spectroscopy, Particle Size Analysis, Scanning Electron Microscopy (SEM), Diffuse Reflectance Spectroscopy (DRS) and Photo Luminescence (PL) Spectroscopy techniques. All the samples were crystallized in cubic structure. Effect of surfactants in the synthesis of nickel oxide (NiO) particles is discussed and reported.
Keywords
Thermal assisted reflux condensation method; NiO nanoparticles; Effect of surfactants
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